KMID : 0881720090240030211
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Journal of Food Hygiene and Safety 2009 Volume.24 No. 3 p.211 ~ p.216
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4,4`-Diaminodiphenylmethane Migration from Nylon Kitchen Utensils using LC-MS/MS
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Eom Mi-Ok
Yoon Hae-Jung Choi Hyun-Chul Jeon Dae-Hoon Kim Hyung-Il Sung Jun-Hyun Park Na-Young Lee Eun-Joon Lee Young-Ja
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Abstract
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In order to cope with risk issues of overseas on 4,4¡¯-diaminodiphenylmethane (4,4¡¯-MDA) known to used in the production of polyamide resins, we investigated on 4,4¡¯-MDA migration from plastic cooking utensils. 93 samples of plastic cooking utensils were collected from the retail markets in 7 major cities of Korea during March to June, 2007 and 4,4¡¯-MDA levels migrated to food simulants, water, 4% acetic acid, 20% ethanol and n-heptane, on plastic cooking utensils was quantified by liquid chromatography with tandem mass spectrometry (LC-MS/MS). 4,4¡¯- MDA was detected in 14 samples, and the levels of 4,4¡¯-MDA migrated to food simulants were in the range of 0.001 ~ 0.026 ppm. Among them, the 4,4¡¯-MDA migration amounts of 2 samples were above 0.01 ppm defined by the EU.
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KEYWORD
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4,4`-MDA, PAAs, nylon, utensils, migration
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